http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107501366-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07H1-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07H17-07 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H1-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H17-07 |
filingDate | 2017-08-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2020-08-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2020-08-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-107501366-B |
titleOfInvention | A kind of method for purifying troxerutin from troxerutin waste liquid powder |
abstract | The invention discloses a method for purifying troxerutin from troxerutin waste liquid powder. Step 2, sample loading: dissolve the troxerutin waste liquid powder with an eluent, and load the sample by wet method; step 3, elution: carry out the troxerutin waste liquid powder after wet loading in step 2. Elution, TLC analysis and detection, then collect the eluate A containing Troxerutin, concentrate under reduced pressure to obtain Troxerutin crude fraction; Step 4, dissolve the Troxerutin crude fraction obtained in Step 3 After the membrane is further separated and purified by semi-preparative high performance liquid chromatography, the eluate B containing Troxerutin is collected, concentrated under reduced pressure, and freeze-dried to obtain brown-yellow Troxerutin powder. In the present invention, the troxerutin waste liquid powder is treated by a silica gel chromatography column combined with a purification method of semi-preparative high performance liquid chromatography, and the troxerutin content reaches 98%. |
priorityDate | 2017-08-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 36.