http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107488447-B

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filingDate 2017-09-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2019-08-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2019-08-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-107488447-B
titleOfInvention A kind of preparation of core-shell type magnetic multicolor fluorescence probe and visible detection method
abstract The invention belongs to nanocomposite preparation technical fields, and in particular to a kind of preparation of core-shell type magnetic multicolor fluorescence probe and visible detection method.The wherein preparation of rear-earth-doped core-shell type magnetic multicolor fluorescence probe, including three steps: (1) allowing fluorescein to load on magnetic halloysite with hydro-thermal method, at this point, magnetic kaolin will show green fluorescence under ultraviolet analysis instrument for three purposed;(2) fluorescein is leaked out of magnetic halloysite in order to prevent, and using APTES+TEOS mixed liquor, ammonium hydroxide is added dropwise, and react the hydroxyl for allowing amino to replace product, to form layer protecting film;(3) edetic acid derivatives are next grafted, and then form chelating object with rare-earth ion coordination, fluorescence probe is made.It is additionally related to a kind of visible detection method, fluoremetry is carried out to the detected material DPA of various concentration after above-mentioned fluorescence probe is mixed with Tris-HCl buffer solution, obtains the recognition performance that multicolor fluorescence variation illustrates the fluorescence probe.
priorityDate 2017-09-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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