http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107382795-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_a7e9119bf73632a42c8e27d6d92dd61b |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C303-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C303-44 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C303-38 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C311-48 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C303-44 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C303-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C303-38 |
filingDate | 2017-08-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_09f99572fceb0ce64dd15e406b1a1c58 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c8377f91c383bf783a3cef2edc5571f4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b502760546b38097bfa25cfa05198479 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_712201d29791d56e84f34b14944da069 |
publicationDate | 2017-11-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-107382795-A |
titleOfInvention | A kind of method of synthesizing perfluoroalkyl sulfimide salt |
abstract | The invention discloses a kind of method of synthesizing perfluoroalkyl sulfimide salt of technical field of chemical synthesis, this method specifically comprises the following steps:S1:Trifluoromethanesulfonic acid is reacted with liquefied ammonia;S2:Filtered after vibration dissolving and obtain waxy solid C 4 F 9 SO 2 NH 2 Crude product;S3:C is made 4 F 9 SO 2 NH 2 Highly finished product;S4:By C 4 F 9 SO 2 NH 2 Highly finished product sublimator;S5:Add lytic agent dissolving C 4 F 9 SO 2 NH 2 ;S6:It is layered in separatory funnel;S7:1~2g of carbonate is weighed to be added thereto and then filter, rotate and obtain per-fluoroalkyl sulfonyl inferior amine salt solid after being dried under reduced pressure;S8:Per-fluoroalkyl sulfonyl inferior amine salt highly finished product are obtained, preparation method of the present invention is simple, high income, and the addition product in building-up process can be recycled recycling, high financial profit, the purity height of its per-fluoroalkyl sulfonyl inferior amine salt prepared. |
priorityDate | 2017-08-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 45.