http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107365278-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_b0b24935b727dd8d91af84b6e0077a06 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D261-20 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D261-02 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D261-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D261-20 |
filingDate | 2017-06-09-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_40f6e748de832235a8eba59e39b062ea http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e4c1147c970d21d9dbe170f09387cc06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7987134e03cc42925a1be8c79265624e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8146cf778c42dcec1bebcb9c99bc08a2 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0996498179c66b7f0f6e597804edd75a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_93363993a31225e4102a54a999dcdd03 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_463da670a17b4ece09db37e46f3a9306 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_aca26af6712564d63b0d3233cabe090f http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_889d41a8e9365febd8f0368a24ddc866 |
publicationDate | 2017-11-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-107365278-A |
titleOfInvention | A kind of polysubstituted isoxazolidine derivative and its preparation method |
abstract | The invention relates to a multi-substituted isoxazolidine derivative and a preparation method thereof, the structural formula of which is shown in formula (I): Formula (I), wherein, R 1 and R 2 are substituted aryl or alkyl, and the substituent on Ar can be alkoxy, halogen or alkyl; the substituted aryl is phenyl or naphthyl, and the alkyl Usually include: methyl, ethyl, cyclohexyl, the preparation method steps are as follows: at room temperature, under air or nitrogen atmosphere, the nitrone derivative shown in formula (II), the nitrone derivative shown in formula (III) containing alkene structure The compound and the photocatalyst represented by formula (IV) are dissolved in an organic solvent, mixed uniformly, placed under a blue LEDs lamp or an incandescent lamp for several hours, and after the reaction is complete, the solvent is evaporated, and then separated by silica gel column chromatography Purification can obtain multi-substituted isoxazolidine derivatives; this method solves the problem that the existing synthesis of isoxazolidine derivatives requires a high-temperature heating system, high energy consumption, harsh conditions, and great requirements for equipment. The conditions are mild, the method is simple and The operation is convenient and the productivity is high. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107746392-B http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109796422-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109796422-B http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107746392-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112939883-A |
priorityDate | 2017-06-09-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 30.