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filingDate 2017-07-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2019-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2019-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-107162048-B
titleOfInvention A kind of preparation method of titanium dioxide/nitridation carbon composite nano-material
abstract A kind of preparation method of titanium dioxide/nitridation carbon composite nano-material, comprising the following steps: S1:, which weighing, or measures carbon source, nitrogen source, oleic acid is added in three-necked flask;S2: installing and be heated to reflux device, under room temperature magnetic agitation by titanium source be added step S1 in three-necked flask in after carry out heating reaction, start timing when reaction system comes to life, after 10-50 minute stop heating and remove heat source;S3: after the reaction system cooled to room temperature after heating in step S2, supernatant liquid is removed, collects precipitated product;S4: the precipitated product obtained in step S3 is sufficiently washed, and the product after washing is 5-8 hours dry under 20-50 DEG C of vacuum condition;Dry to terminate to obtain titanium dioxide/nitridation carbon composite nano-material, the titanium dioxide/nitridation carbon composite nano-material is water-soluble titanium dioxide/nitridation carbon composite nano-material.The problem of preparation method of the present invention solves prior art operation complex steps, and time-consuming.
priorityDate 2017-07-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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