http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107102082-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-72 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-72 |
| filingDate | 2017-05-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2019-12-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2019-12-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-107102082-B |
| titleOfInvention | Method for determining residual quantity of amitraz and metabolite thereof in royal jelly by liquid chromatography-mass spectrometry/mass spectrometry |
| abstract | The invention relates to a method for detecting amitraz and metabolite residues thereof in royal jelly, in particular to a method for simultaneously determining amitraz, 2,4-dimethyl benzamide and 2,4-dimethyl aniline in royal jelly by liquid chromatography-tandem mass spectrometry. A method for determining residual quantities of amitraz and metabolites thereof in royal jelly by liquid chromatography-mass spectrometry/mass spectrometry comprises the steps of diluting a sample by ammoniated water, precipitating and extracting protein by ammoniated acetonitrile, purifying an extracting solution by a neutral alumina solid phase extraction column, detecting by liquid chromatography-mass spectrometry/mass spectrometry, quantifying by an internal standard method of amitraz and 2,4-dimethylaniline, and quantifying by an external standard method of monoamitraz and 2,4-dimethyl phenyl formamide. The sensitivity of the method can meet the detection and confirmation requirements of the residual quantity of amitraz and metabolites thereof in royal jelly. |
| priorityDate | 2017-05-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 78.