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filingDate 2017-06-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_36c43e1955018a40ea5f34a01566d0c9
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publicationDate 2017-08-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-107085064-A
titleOfInvention The high performance liquid chromatography tandem mass spectrum Simultaneous Detection of acetic acid fusarinine C and double methyl mercapto gliotoxins in sputum
abstract The invention provides acetic acid fusarinine C (TAFC) in a kind of sputum and the high performance liquid chromatography tandem mass spectrum Simultaneous Detection of double methyl mercapto gliotoxins (bmGT), step is as follows:(1) preparation of standard specimen and sample;(2) each standard specimen and sample obtained by step (1) are measured using liquid chromatography tandem mass spectrometry, obtain standard specimen and sample spectrogram, record the peak area of TAFC, bmGT and phenacetin in each standard specimen and sample spectrogram;(3) TAFC and bmGT working curve is drawn, the concentration of TAFC and bmGT in sample is calculated according to the peak area ratio and working curve of the peak area ratio of TAFC and phenacetin, bmGT and phenacetin in sample spectrogram.The present invention is detected while realizing from sputum to TAFC and bmGT, and new approach is provided for TAFC and bmGT detection, is conducive to improving detection efficiency.
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