http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107056590-B

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C41-40
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C41-24
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-40
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-24
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C43-225
filingDate 2017-05-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-11-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-11-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-107056590-B
titleOfInvention Industrial method for preparing and purifying 4, 4' -dimethoxy triphenylchloromethane
abstract The invention discloses an industrial method for preparing and purifying 4, 4' -dimethoxytriphenylchloromethane, which takes anisole and trichlorotoluene as initial raw materials to prepare a DMT-Cl crude product through an F-C reaction, a hydrochloric acid hydrolysis reaction and a chlorination reaction, wherein the purity of the DMT-Cl crude product is more than 98.5 percent, the DMT-Cl crude product is crystallized by a solvent to obtain a DMT-CL finished product with the purity of more than 99.9 percent, and the yield of the DMT-CL finished product is more than 80 percent. The industrial method for preparing and purifying the 4, 4' -dimethoxy triphenylchloromethane has reasonable design, can avoid using a format reagent and a more expensive refined solvent, achieves the aim of producing the DMT-CL with high purity in a safe, environment-friendly and industrialized way, and meets the high-quality standard of biological nucleoside and nucleotide.
priorityDate 2017-05-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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