http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107056590-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C41-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C41-24 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-24 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C43-225 |
filingDate | 2017-05-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2020-11-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2020-11-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-107056590-B |
titleOfInvention | Industrial method for preparing and purifying 4, 4' -dimethoxy triphenylchloromethane |
abstract | The invention discloses an industrial method for preparing and purifying 4, 4' -dimethoxytriphenylchloromethane, which takes anisole and trichlorotoluene as initial raw materials to prepare a DMT-Cl crude product through an F-C reaction, a hydrochloric acid hydrolysis reaction and a chlorination reaction, wherein the purity of the DMT-Cl crude product is more than 98.5 percent, the DMT-Cl crude product is crystallized by a solvent to obtain a DMT-CL finished product with the purity of more than 99.9 percent, and the yield of the DMT-CL finished product is more than 80 percent. The industrial method for preparing and purifying the 4, 4' -dimethoxy triphenylchloromethane has reasonable design, can avoid using a format reagent and a more expensive refined solvent, achieves the aim of producing the DMT-CL with high purity in a safe, environment-friendly and industrialized way, and meets the high-quality standard of biological nucleoside and nucleotide. |
priorityDate | 2017-05-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 53.