http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107029759-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D213-53 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D307-52 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D317-58 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C249-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C251-24 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J27-13 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D213-53 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D317-58 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J27-13 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C249-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D307-52 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C251-24 |
| filingDate | 2016-02-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2019-11-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2019-11-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-107029759-B |
| titleOfInvention | Ruthenium trichloride reacts the application prepared in imines with alcohol compound in catalysis nitrobenzene compounds |
| abstract | The invention discloses a kind of ruthenium trichlorides to react the application prepared in imine compound with alcohol compound in catalysis nitrobenzene compounds.Specifically; this method comprises the following steps: under inert gas protection; according to nitrobenzene compounds: alcohol compound: alkali compounds: ruthenium trichloride=1:2 ~ 4:1 ~ 2:0.02 ~ 0.05 molar ratio; above-mentioned reactant is added in the reaction vessel for being equipped with agitating device; it is stirred to react in 100 ~ 150 DEG C 20 ~ 30 hours, obtains imine compound.The present invention in the case where not adding any assistant ligand and solvent, directly uses RuCl for the first time 3 As catalyst.In addition, the present invention realizes the selectivity preparation of imine compound, whole process is green, efficient and easily operated, is a kind of good method of synthesizing imine class compound. |
| priorityDate | 2016-02-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 71.