http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106966966-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_4baf61b82705468dd1ff913b8ce785f7 |
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07B2200-13 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D213-77 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D213-77 |
filingDate | 2017-04-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_52317fed040bae1707d618b06c92cc33 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_50a21ac0e35be37fcd61430c84227ef9 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_665de77f90b8f5a5690dd55e70e9719d |
publicationDate | 2017-07-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-106966966-A |
titleOfInvention | A kind of 3,5 Dibromosalicylaldehydes contracting hydrazino pyridine Schiff base zinc complex of 2 chlorine 6 and synthetic method |
abstract | A kind of 3,5 Dibromosalicylaldehydes contracting 2 chlorine 6 hydrazino pyridine Schiff base zinc complex [Zn (dbcp) 2 ]·DMF·H 2 O and synthetic method.The Zn complex [Zn (dbcp) 2 ]·DMF·H 2 O molecular formula is:C 24 H 14 Br 4 Cl 2 N 6 O 2 Zn·C 3 H 7 NO·H 2 O, molecular weight is:964.43g/mol, Hbhdp are the 3,5 Dibromosalicylaldehydes contracting hydrazino pyridine schiff bases of 2 chlorine 6.By 2.977g analytically pure 3,5 Dibromosalicylaldehydes, the analytically pure hydrazino pyridines of 2 chlorine 6 of 1.436g are dissolved in 30mL analysis straight alcohol solution, part Hdbcp are obtained after being heated to reflux two hours.Dried 0.202 0.404g Hdbcp are dissolved in 5 10mL and analyze pure DMF, 0.149 0.298g analyzes pure zinc nitrate hexahydrate and is dissolved in 5 10mL redistilled waters, it is placed in reactor, three days is stood in 80 DEG C of baking ovens, has yellow web crystal to generate i.e. [Zn (dbcp) 2 ]·DMF·H 2 O.Present invention process is simple, with low cost, chemical constituent is easily controllable, reproducible and yield is high. |
priorityDate | 2017-04-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 38.