http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106966933-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C327-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D277-74 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D295-26 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C319-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D295-135 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D295-096 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C319-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D295-096 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-38 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C327-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-37 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D295-26 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-20 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D277-74 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D295-135 |
filingDate | 2017-03-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2019-01-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2019-01-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-106966933-B |
titleOfInvention | A kind of method of synthesizing aryl thio-ether type compounds |
abstract | The present invention provides a kind of methods of synthesizing aryl thio-ether type compounds, the following steps are included: phenolic compound or aminated compounds, sulfur alcohol compound, transition-metal catalyst, water are added in reaction flask, sealing, oxygen, heating stirring reaction are filled with into reaction flask, after through extraction, drying, concentration, purifying, aryl thioethers class compound is made.The present invention provides a kind of to be catalyzed the oxidative coupling reaction of phenols or aminated compounds and sulfur alcohol compound by phthalocyanines transition-metal catalyst to prepare the new method of aryl thioethers class compound.Synthesis step is simple, easy to operation, product yield high, and up to 80% or more, the synthesis for aryl thioethers class compound provides a kind of new way.With existing method ratio, raw material is cheap and easy to get, and with water as solvent (catalyst can be well dissolved in water), under heterogeneous conditions, can obtain aryl thioether compound of the high score from yield, improve the efficiency of reaction and the Atom economy of reaction. |
priorityDate | 2017-03-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 44.