http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106966844-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C06B33-04 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C06B33-04 |
filingDate | 2017-02-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2018-11-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2018-11-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-106966844-B |
titleOfInvention | Graphene-based carbohydrazide metal complex crystal energetic material and preparation method thereof |
abstract | The invention discloses the preparation methods of graphene-based carbohydrazide metal complex crystal energetic material, include the following steps:The graphene oxide of oxygen content >=45% is distributed in water or organic solvent, disperses 30~60min, obtains graphene oxide suspension;Under the conditions of temperature is 55~65 DEG C, graphene oxide suspension is reacted with coupling agent, the reaction time is 1.5~2h, obtains graphene oxide activation presoma;Graphene oxide activation presoma is distributed in dispersing agent one, disperses 30-50min, carbohydrazide is added, under the conditions of 60~70 DEG C, 4h is reacted, obtains the graphene oxide of carbohydrazide functionalization;After the graphene oxide cleaning filtering of the carbohydrazide functionalization in S3, it is distributed in dispersing agent two, disperse 15~60min, phosphinylidyne hydrazine solution is added, nitrate or perchlorate are added, at 75~85 DEG C, reacts 15~60min, after vacuum drying, graphene-based carbohydrazide metal complex crystal energetic material is obtained;Solve the problems, such as that laser ignition low efficiency, the preparation process of photosensitive insensitive energetic material are complicated. |
priorityDate | 2017-02-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 78.