http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106946883-B

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D471-04
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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D471-10
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D471-04
filingDate 2017-03-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2019-04-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2019-04-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106946883-B
titleOfInvention With the alkaloid compound and preparation method of the type skeleton of dimeric piperidine I and II in its root of arna
abstract The present invention relates to, with the alkaloid compound and preparation method of the type skeleton of dimeric piperidine I and II, have the alkaloid compound 1 of I type skeleton (I) of dimeric piperidine class are as follows: 2,2,4,5 in a kind of its root of arna, 7,7,8a- seven methyl -2,6,7,8,8a, 9- hexahydro -3 H Cyclopenta [1,2- b :3,4‑ c '] double pyridine -3- ketone;Alkaloid compound 2 with II type skeleton (II) of dimeric piperidine class are as follows: 3a 1 Seven methyl -2,3a of hydroxyl -2,2,5,7,7,10,10- 1 , 7,8,10,11- hexahydro -9 H Pyrido [4', 3':3,4] cyclopenta [1,2,3- de ] quinoline -4 (6 H ) -one;It is extracted using the mixed solvent of acetone/methanol, total alkali is obtained by the heavy legal system of the molten alkali of acid, ethyl acetate extract is obtained by solvent distribution method, recycles the isolated alkaloid compound 1 and compound 2 with the type skeleton of dimeric piperidine I and II of RP chromatography.
priorityDate 2017-03-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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