http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106920946-B

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filingDate 2017-04-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-11-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-11-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106920946-B
titleOfInvention Preparation method of aluminum oxide and carbon composite coated sodium vanadium fluorophosphate cathode material
abstract The invention provides an alumina and carbon composite coated sodium vanadium fluorophosphate cathode material and a preparation method thereof, wherein oxalic acid H is used 2 C 2 O 4 Dissolving sodium fluoride NaF, a vanadium source and a phosphorus source in deionized water, stirring at 60 ℃ to form gel, drying, and presintering the powder in a tube furnace to obtain a precursor; adding a carbon source into the precursor, performing ball milling, drying, calcining in a tubular furnace under the nitrogen atmosphere, and sieving to obtain a carbon-coated sodium vanadium fluorophosphate cathode material; ultrasonically dispersing carbon-coated sodium vanadium fluorophosphate in deionized water uniformly, and adding aluminum nitrate Al (NO) nonahydrate 3 ) 3 ·9H 2 O ultrasonic treatment for 20 min, stirring for 30 min, and adding ammonia NH 3 ·H 2 And O, continuously stirring for 1.5 hours at the temperature of 60 ℃, then carrying out suction filtration, washing for multiple times by using deionized water, drying, finally carrying out final firing in a tubular furnace, cooling, and sieving to obtain the aluminum oxide and carbon composite coated sodium vanadium fluorophosphate cathode material.
priorityDate 2017-04-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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