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filingDate 2017-03-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2019-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2019-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106905480-B
titleOfInvention A kind of preparation method of 1,2,3,4,6- O-Penta-O-galloyl-D-glucopyranose molecular engram integral column
abstract The present invention relates to one kind 1, 2, 3, 4, the preparation method of 6-O- Penta-O-galloyl-D-glucopyranose molecular engram integral column, this method is with 1, 2, 3, 4, 6-O- Penta-O-galloyl-D-glucopyranose is template molecule, with ternary pore-foaming agent N, dinethylformamide, dimethyl sulfoxide and 1- butyl -3- methyl tetrafluoroborate make solvent, add function monomer, crosslinking agent, metal ion, methyl ether methacrylate oligomer and initiator, then ultrasonic dissolution and inflated with nitrogen removal dissolved oxygen, polymerization reaction is carried out in a water bath, finally obtain selective 1, 2, 3, 4, 6-O- Penta-O-galloyl-D-glucopyranose molecular engram integral column.The method of the invention imprinting factor is big by 73.9, can be used for Solid Phase Extraction, realizes the characteristic selective purification to 1,2,3,4,6-O-pentagluacyl glucose.Imprinted polymer preparation is simple, and durability is good, as the filler of Solid Phase Extraction, provides a kind of effective method for isolate and purify (purity is greater than 98%) of 1,2,3,4,6-O-pentagluacyl glucose.
priorityDate 2017-03-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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