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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C37-055
filingDate 2017-01-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_90f21f730dce87255922a30e85caba2b
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8dd63ad9ba718810aadd76b8ecf65ec6
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publicationDate 2017-06-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106866378-A
titleOfInvention A kind of synthetic technique of phloroglucinol
abstract The invention belongs to the technical field of medicine production, and in particular relates to a synthesis process of phloroglucinol. The synthetic technique of phloroglucinol of the present invention takes 1,3,5-trimethoxybenzene as raw material, takes chlorobenzene as solvent, aluminum trichloride as complexing reagent, heating reaction; Dissociate in aqueous solution and filter; the crude product is recrystallized in a mixed solvent of alcohol and water to obtain high-purity phloroglucinol in a higher yield. The method has the advantages of simple operation, strong controllability, and suitable for large-scale production.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113527064-A
priorityDate 2016-12-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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