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filingDate 2017-01-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2019-01-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2019-01-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106865506-B
titleOfInvention It is a kind of to form controllable nickel cobalt compound nano line and the preparation method and application thereof
abstract Controllable nickel cobalt compound nano line and the preparation method and application thereof is formed the invention discloses a kind of, controllable nickel cobalt compound nano line its general formula of the composition are as follows: NiCo 2 (S 1‑x Se x ) 4 , 0 < x < 1;Its pattern is the pearl shape nano wire that multiple little particles are connected into.Preparation method: nickel nitrate, cobalt nitrate and urea are mixed into obtained precursor mixed solution in water;Substrate is transferred in autoclave together with precursor mixed solution and is reacted at 80~150 DEG C 200~400 minutes, NiCo is made 2 (OH)(CO 3 ) 2 Nano wire;To substrate and NiCo 2 (OH)(CO 3 ) 2 Nano wire is dried, then is placed in sulphur powder and selenium powder mixed-powder, and is heated 0.5~2 hour and be cooled to room temperature with 400~500 DEG C in protective gas.The present invention not only has a better electrolysis water catalytic performance, and preparation process it is simple, rapidly and efficiently, it is low in cost, environment friendly and pollution-free, be suitble to large-scale industrial production.
priorityDate 2017-01-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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