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filingDate 2017-01-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2019-06-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2019-06-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106753217-B
titleOfInvention Preparation method of a new type of hot vulcanized liquid silicone rubber
abstract The invention relates to a method for preparing a novel hot vulcanized liquid silicone rubber, which comprises the following steps: (1) under the catalysis of a catalyst, polymerizing D 4 (octamethylcyclotetrasiloxane) and a capping agent to prepare (2) adding monomer A and monomer B into an organic solvent to obtain a monomer mixture; adding the monomer mixture to a hydrolysis medium, and performing a hydrolysis reaction under the catalysis of a hydrolysis catalyst to obtain different electrophiles The silicone resin with group content and fluidity is used as a cross-linking agent; (3) after the base glue, the cross-linking agent and the filler are mixed uniformly, and then cured, a new type of hot vulcanized liquid silicone rubber is obtained. The liquid silicone rubber of the present invention is different from the condensation type, peroxide cross-linking and hydrosilylation cross-linking system of traditional silicone rubber, and the cross-linking mechanism is amine-ene reaction; the product is one-component, can be cured by heating at medium temperature, and can be cured at room temperature. Stable storage; by controlling the ratio of fillers, fluid or thixotropic products can be obtained, which can be used as adhesives or sealants.
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