http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106749727-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_44cdc47edd467be366a4fa7abbe1ea39 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08B37-0003 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08B37-00 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08B37-00 |
filingDate | 2016-12-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_73d4b1f34460797edc4ea17b72ebd5bb |
publicationDate | 2017-05-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-106749727-A |
titleOfInvention | A kind of preparation method of pachyman sulfuric acid ester |
abstract | The present invention relates to a kind of preparation method of pachyman sulfuric acid ester, it is characterised in that comprise the following steps:Weigh 100g Poria cocos powders, it is dissolved in points for 3 times and is total up in 10 times of 0.5mol/LNaoH of volume, every time 4 DEG C of extraction polysaccharide 8h, merges 3 extraction supernatants, 10% acetic acid is neutralized to pH6~7, precipitates overnight in 4 DEG C of refrigerators, in 4 DEG C of environment, 5000g centrifugation 20min, collects precipitation, deionized water washing precipitation 3 times, washed successively 3 times with absolute ethyl alcohol, acetone and ether, in 70 DEG C of dry white pachymarans, smashed stand-by;Pachyman sulfuric acid ester sulfonation efficiency high prepared by the method for the invention, molecular weight is small, and low production cost, environmental pollution are small. |
priorityDate | 2016-12-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 34.