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filingDate 2016-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-07-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-07-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106745534-B
titleOfInvention Composite photocatalytic electrode of photo-reduction metal-modified cobaltosic oxide/titanium dioxide p-n heterojunction and preparation method thereof
abstract The invention discloses a composite photocatalytic electrode of a photo-reduction metal-modified cobaltosic oxide/titanium dioxide p-n heterojunction and a preparation method thereof, wherein (1) a titanium dioxide nanotube is soaked in a silver nitrate or chloroauric acid or chloroplatinic acid solution, stirred for 0.5-1.5 h at normal temperature, inert gas is dried after solid-liquid separation, and ultraviolet light is irradiated for 0.5-2 h to obtain the titanium dioxide nanotube electrode with the surface coated with silver or gold or platinum nanoparticles; (2) soaking the titanium dioxide nanotube electrode prepared in the step (1) in a cobalt acetate glycol solution, then carrying out solid-liquid separation, and sequentially carrying out vacuum drying and calcination treatment to obtain the composite photocatalytic electrode. And (3) applying a bias voltage of 1-3V by using the composite photocatalytic electrode and the titanium sheet as cathodes, and carrying out electrolytic treatment for 1-3 h. The composite electrode has good effects on removing nitrobenzene and reducing chromium.
priorityDate 2016-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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