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publicationDate 2017-05-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106645493-A
titleOfInvention A method for detecting quizalofop-p-ethyl and its metabolite residues in complex matrix
abstract The invention provides a method for detecting quizalofop-p-ethyl and its metabolite residues in a complex matrix. The method is a matrix solid-phase dispersion extraction method, comprising the following steps: (1) extracting residues in a sample; (2) purifying: measuring Take the extract in step (2) and add a purifying agent to carry out solid-phase dispersion extraction of the matrix; (3) configure a standard solution; (4) detect with high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS); (5) establish a standard Curve; (6) Analysis of results. The detection method of the invention can quickly, sensitively and accurately determine the residual amount of quizalofop-p-p-p and its metabolites, and provides a new detection technology for the detection of the herbicide quizalofop-p-p-p-p and its metabolites.
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