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filingDate 2017-01-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2017-05-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106629843-A
titleOfInvention A quaternary ammonium salt-guided method for synthesizing thermally stable layered nanocrystalline zirconia
abstract The invention is a quaternary ammonium salt-guided method for synthesizing thermally stable layered nanocrystalline zirconia. The method comprises the following steps: (1) adding the zirconium oxychloride solution and the quaternary ammonium salt into a reactor with a reflux device, and refluxing for 0.5 to 1 hour to obtain a mixed solution A; (2) adding the sodium hydroxide solution, Add it into the reactor in step (1), and continue to reflux for 1 to 2 hours to obtain a solid-liquid mixture B; (3) move the mixture B into an autoclave, and conduct a hydrothermal reaction at 120-150°C for 13-15 hours to obtain a solid-liquid mixture Mixture C; (4) washing with water, centrifuging, drying, and calcining to obtain a thermally stable layered nanocrystalline zirconia powder. The invention adopts the method of combining "reflux-precipitation-hydrothermal", which not only improves the order degree of the product, but also ensures the good thermal stability of the product.
priorityDate 2017-01-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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