http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106565626-B

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D277-54
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D277-54
filingDate 2016-10-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-06-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-06-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106565626-B
titleOfInvention Synthesis method of 2-amino-4-aryl-5-methylthiothiazole compound
abstract The invention belongs to the technical field of organic chemical synthesis, and relates to a method for efficiently, simply and conveniently synthesizing 2-amino-4-aryl-5-methylthiothiazole compounds. The method comprises the following synthesis steps: (1) dissolving arylethanone in a DMSO/HBr mixed system, and heating to react to obtain alpha-bromoacetophenone dimethyl sulfonium salt; (2) dissolving the sulfonium salt prepared in the step (1) in water, adding thiourea, and stirring at room temperature; then adding ethanol, and continuously heating for reaction to prepare the 2-amino-4-aryl-5-methylthiothiazole.
priorityDate 2016-10-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 49.