http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106565626-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D277-54 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D277-54 |
filingDate | 2016-10-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2022-06-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2022-06-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-106565626-B |
titleOfInvention | Synthesis method of 2-amino-4-aryl-5-methylthiothiazole compound |
abstract | The invention belongs to the technical field of organic chemical synthesis, and relates to a method for efficiently, simply and conveniently synthesizing 2-amino-4-aryl-5-methylthiothiazole compounds. The method comprises the following synthesis steps: (1) dissolving arylethanone in a DMSO/HBr mixed system, and heating to react to obtain alpha-bromoacetophenone dimethyl sulfonium salt; (2) dissolving the sulfonium salt prepared in the step (1) in water, adding thiourea, and stirring at room temperature; then adding ethanol, and continuously heating for reaction to prepare the 2-amino-4-aryl-5-methylthiothiazole. |
priorityDate | 2016-10-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 49.