http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106565513-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C231-02 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C233-18 |
| filingDate | 2016-10-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2019-03-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2019-03-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-106565513-B |
| titleOfInvention | The method for preparing beta-hydroxy alkylamide using microwave heating |
| abstract | It is prepared using microwave heating β The method of hydroxyalkyl amide is related to preparing β The method of hydroxyalkyl amide is prepared the present invention provides a kind of β The method of hydroxyalkyl amide, connects microwave device, and installation 250mL volume three-necked flask is put into magnetic rotor in cavity, three-necked flask is connected to atmosphere.Diethanol amine, catalyst, ester, polar solvent is added, stirs evenly.It opens microwave heating equipment, preset heating power, temperature, time respectively, open stirring, open function heating schedule；Reach preset time to microwave heating equipment, stop heating, stops stirring, three-necked flask is taken out.After placing room temperature, crystallization obtains white solid.It crushes, it is spare.The present invention makes the reaction time at least shorten three times, and easy to operate, temperature control is accurate, and side reaction is few, and yield is high, environmental-friendly. |
| priorityDate | 2016-10-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 50.