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filingDate 2016-10-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2019-01-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2019-01-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106540723-B
titleOfInvention A kind of preparation method of thiophosphoric acid silver catalyst
abstract The present invention discloses a kind of preparation method of thiophosphoric acid silver catalyst, in turn includes the following steps: by 50~60g thiophosphoryl chloride (PSCl 3 ), it is added in 300~400mL sodium hydroxide solution, wherein 100~120g containing sodium hydroxide, is heated to reflux until PSCl 3 It is completely dissolved;100mL ethyl alcohol is added after cooling is placed in 6~8h in ice-water bath;The product of precipitation is separated by solid-liquid separation, and solid is dissolved in 90~120mL water at 50~60 DEG C, 20~35g silver nitrate is added, is cooled to room temperature, filters, solid is dried, a kind of thiophosphoric acid silver catalyst can be obtained.The catalyst has preferable crystal structure, stablizes, and have the absorption region of wider light.
priorityDate 2016-10-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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