http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106478423-B

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C209-08
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C211-08
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C209-08
filingDate 2016-10-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2018-10-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2018-10-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106478423-B
titleOfInvention Synthesize N, the method for N- diisopropylethylamine
abstract The invention discloses a kind of synthesis N, the method for N diisopropylethylamine, using quaternary ammonium salt as ethylating agent, using alcohol as solvent, synthesizes N, N diisopropylethylamine using diisopropylamine as reaction raw materials in the presence of acid binding agent;Diisopropylamine:Quaternary ammonium salt=1:1~2 molar ratio, back flow reaction 3~7 hours;The reaction product of gained is post-treated, obtains the N of high-purity, N diisopropylethylamine.Method synthesis DIPEA using the present invention has many advantages, such as that easy to operate, yield is higher, post-processing is simple.
priorityDate 2016-10-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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