http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106478327-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C201-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C255-50 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-32 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-09 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07B43-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C253-30 |
| filingDate | 2015-08-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2019-05-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2019-05-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-106478327-B |
| titleOfInvention | A kind of method of synthesizing (nitroalkynyl) benzene compounds |
| abstract | The invention provides a method for a (nitroalkynyl) benzene compound shown in formula II: the phenylacetylene compound shown in formula I is used as a raw material, and a nitrating reagent is added to an organic solvent, and the temperature is sealed at 20-50° C. The reaction is carried out at a temperature, followed by TLC until the end of the reaction, and the reaction solution is post-treated to obtain the (nitroalkynyl) benzene compound represented by formula II. The nitration method of the invention has the advantages of specificity of the nitration position, only nitration on the alkynyl group, without the formation of nitration products on the benzene ring, the reaction process is safe and environmentally friendly, the substrate adaptability is good, and various substituents can realize the alkyne base nitration. |
| priorityDate | 2015-08-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 73.