http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106477578-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B32-914 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B32-921 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B32-90 |
| filingDate | 2015-08-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2018-09-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2018-09-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-106477578-B |
| titleOfInvention | A kind of MXene two-dimensional material preparation methods based on acid deep co-melting solvent |
| abstract | The present invention relates to a kind of two-dimensional material preparation method, a kind of MXene two-dimensional material preparation methods based on acid deep co-melting solvent include the following steps：1, the co-melting solvent of depth and MAX phases constituted by the co-melting solvent of the depth being made of Hydrogen Bond Acceptors and hydrogen-bond donor with MAX phases or by Hydrogen Bond Acceptors, hydrogen-bond donor and fluoride, it is added in reactor and carries out 1~72h of mixing, mixing speed is controlled in 200~2000rpm, at 20~70 DEG C, the molar ratio of Hydrogen Bond Acceptors and hydrogen-bond donor is 1.0 for temperature control：1.0~4.0, the molar ratio of Hydrogen Bond Acceptors and fluoride is 1.0：The mass ratio of 0~1.0, MAX phase and deep co-melting solvent is 1.0：20~200.2, the reaction solution for obtaining step 1 uses deionized water to be washed to pH value as 5~7, and further carries out centrifugal treating to it, under protection of argon gas, is placed in 0.5~1h of ultrasound in isopropanol, then filter 0.5~1h with ethyl alcohol, MXene two-dimensional materials are made.Operating condition of the present invention is mild, synthesis technology is simple, environmental-friendly and material purity is higher, can largely prepare synthesis. |
| priorityDate | 2015-08-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 53.