http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106432016-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C319-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C319-28 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C321-28 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C319-14 |
| filingDate | 2016-09-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2018-01-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2018-01-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-106432016-B |
| titleOfInvention | A kind of method for synthesizing THIOANISOLE |
| abstract | The present invention relates to a kind of method for synthesizing THIOANISOLE, using benzenethiol sodium as reaction raw materials, quaternary ammonium salt is as methylating reagent, and alcohol is as solvent.The mol ratio of benzenethiol sodium and the quaternary ammonium salt is 1: 1~1: 5, and the mass ratio of benzenethiol sodium and the alcoholic solvent is 1: 1~1: 10, and reaction temperature is 50 DEG C~180 DEG C, and the reaction time is 2~24 hours.After the completion of reaction, removed under reduced pressure solvent, reactant mixture is washed with water, collects oil phase, rectification under vacuum, collect (10mmHg, 67 69 DEG C) cut. |
| priorityDate | 2016-09-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 44.