http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106431831-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C29-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C41-30 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C45-69 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C45-42 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C33-025 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C29-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-145 |
| filingDate | 2016-09-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2018-12-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2018-12-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-106431831-B |
| titleOfInvention | A kind of synthetic method of 5E- decene-1-alcohol and acetic acid 5E- ubidecarenone |
| abstract | The present invention provides the synthetic methods of a kind of 5E- decene-1-alcohol and acetic acid 5E- ubidecarenone, using methacrylaldehyde and acetylene as raw material, coupling reaction occurs under the conditions of existing for the palladium catalyst and obtains the bromo- 4E- pentenals of 5-, the bromo- 4E- pentenals of 5- carry out Wittig with methoxymethyl triphenylphosphonium phosphonium chloride and react to obtain 1E, 5E-1- bromine 6- methoxyl group hexadiene, Kumada coupling reaction, which is carried out, with butyl magnesium bromide again obtains 1E, 5E-1- methoxyl group decadinene, hydrolysis obtains 5E- decenal, it restores to obtain 5E- decene-1-alcohol, obtains acetic acid 5E- ubidecarenone after being finally esterified.Synthesis material of the invention is cheap and easy to get, and synthetic route is simple, and reaction condition is mild, and convenient and safe operation is easy to industrialized production, and yield is high, is of great significance to the prevention and treatment of anarsialineatella. |
| priorityDate | 2016-09-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 131.