http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106397354-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07B2200-13 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D285-135 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D285-135 |
filingDate | 2016-08-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2018-06-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2018-06-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-106397354-B |
titleOfInvention | A kind of method for improving tebuthiuron crystal mobility |
abstract | The invention belongs to pesticide field more particularly to a kind of methods for improving tebuthiuron crystal mobility, it is characterised in that include the following steps:Tebuthiuron and organic solvent are mixed to form suspension, suspension then is warming up to tebuthiuron is completely dissolved, and obtains tebuthiuron solution;The tebuthiuron solution is carried out to the decrease temperature crystalline of first stage, tebuthiuron solution is cooled to 25 ~ 30 DEG C, after being down to assigned temperature with 12 ~ 20 DEG C/h of speed, stands 5 ~ 60min of heat preservation;The tebuthiuron solution to cool down through the first stage is carried out to the decrease temperature crystalline of second stage, tebuthiuron solution is cooled to 15 ~ 10 DEG C with 25 ~ 30 DEG C/h of speed, after being down to assigned temperature, tebuthiuron crystal is obtained by filtration after standing 0.5 ~ 6h of heat preservation, mother liquor continues to apply mechanically;The granularity of the tebuthiuron crystal is D90:280 ~ 350 microns.The beneficial effects of the present invention are the tebuthiuron crystal obtained by the method for the present invention, granularity D90:280 ~ 350 microns, there is good crystal mobility so that tebuthiuron product has good anticaking capacity. |
priorityDate | 2016-08-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 37.