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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-48
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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-618
filingDate 2015-06-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_67129208471dd44d606ee7ce0a1127e1
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f3ce1867291c8e58645eee3526c9e10c
publicationDate 2017-01-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-106316854-A
titleOfInvention Method for preparing high-content food standard product phenethyl cinnamate
abstract The invention relates to a method for preparing a high-content food standard product phenethyl cinnamate. The method comprises the following steps: performing gas chromatographic analysis on a food-grade phenethyl cinnamate raw material by using an ethanol solution with amount being 10% of the amount of the raw material so as to test that the content of the raw material is greater than or equal to 96%, and performing nature determination, and confirming that main impurities of the raw material are trace ethyl cinnamate, phenethyl alcohol and cinnamic acid; adding the food-grade phenethyl cinnamate into a sodium chloride saturated solution, performing heating under stirring to 80-90 DEG C, performing stirring for 30-45 minutes, and allowing the stirred material to stand for 10-15 minutes; and performing washing, drying and crystallization, thereby obtaining the high-content food standard product phenethyl cinnamate. A phenethyl cinnamate standard product of which the content is 99.6 is prepared from the food-grade phenethyl cinnamate of which the content is only 96% by using a simplified purification technique, and a very fine and complete purification method is provided.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107376620-A
priorityDate 2015-06-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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