http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106220646-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D501-22 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D501-22 |
filingDate | 2016-07-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2018-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2018-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-106220646-B |
titleOfInvention | A kind of method of enzymatic clarification cefalexin mother liquor recycled |
abstract | The invention discloses a kind of methods of enzymatic clarification cefalexin mother liquor recycled, and include the following steps:1)Under certain temperature, with acid solution adjusting cefalexin mother liquor to pH value to 2.0 ~ 3.0;2)Above-mentioned mother liquor is adsorbed, is washed, desorption operation, obtains the solution after desorption;3)Solution after obtained desorption is crystallized with ammonium hydroxide, is filtered, washed, is dried cefalexin finished product;4)By step 3)In filtrate decompression distillation;5)By the disposing mother liquor after the above-mentioned ethyl alcohol distilled and distillation, the dissolving of preparation and preceding 7 ADCA of synthesis for next strippant.Preparation method this method of the present invention is easy to operate, of low cost, energy conservation and environmental protection;Meanwhile using cefalexin made from the method for the present invention compared to the yield higher for not recycling cefalexin made from mother liquor. |
priorityDate | 2016-07-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 28.