http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106187840-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C323-22 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-22 |
filingDate | 2016-07-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-10-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-10-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-106187840-B |
titleOfInvention | A kind of indanone compounds with trifluoromethylthio and preparation method thereof |
abstract | The invention discloses a kind of preparation method of the indanone compounds with trifluoromethylthio, this method chooses acetylenic ketone compounds and fluoroform sulfane alcohol silver compound is raw material, oxidant is used as using persulfate reagent, using HMPA as stabilizer, in reaction dissolvent, in reaction temperature be 80 o Reacted under C, react 12h, reaction obtains indanone compounds after terminating through post processing, the preparation method, which is solved, solves the technical barrier that amide-type and heterocycle directly generate indanone compounds, and the preparation method have it is economical save money, stability is high, reaction condition is gentle, the reaction time is short, raw material is cheap and easy to get, product yield and many advantages, such as high purity. |
priorityDate | 2016-07-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 53.