http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106008221-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C201-12 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-11 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C201-12 |
| filingDate | 2016-06-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2019-04-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2019-04-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-106008221-B |
| titleOfInvention | A kind of synthetic method of adjacent nitro benzyl chloride |
| abstract | The invention discloses a kind of synthetic methods of adjacent nitro benzyl chloride, catalyst, heating stirring are added in ortho-methylnitrobenzene, and be slowly introducing chlorine, to after reaction, recycle ortho-methylnitrobenzene, obtain adjacent nitro benzyl chloride.The defects of the present invention overcomes yield is small, by-product is more existing for thermal chlorination in existing adjacent nitro cylite synthetic method and luminescence method, catalyst is added in ortho-methylnitrobenzene, chlorine is passed through after heating stirring, to after reaction, it is recycled ortho-methylnitrobenzene, adjacent nitro benzyl chloride is obtained, which can get the product (in terms of the ortho-methylnitrobenzene of actual consumption) of purity >=99% and yield >=80%, be higher than thermal chlorination and light chlorination process. |
| priorityDate | 2016-06-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 49.