http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105926021-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02E60-36 |
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J27-1853 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C25B1-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C25D11-34 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B25-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C25B11-04 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C25B1-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C25B11-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B25-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J27-185 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C25D11-34 |
| filingDate | 2016-03-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2018-02-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2018-02-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-105926021-B |
| titleOfInvention | A kind of nickel phosphide nano thin-film and its preparation method and application |
| abstract | The invention discloses a kind of preparation method of nickel phosphide nano thin-film, step are as follows：（1）Dried after nickel foam is cleaned；（2）By step（1）Nickel foam after middle cleaning-drying, with DC stable power supply, in oxalic acid solution, carries out anodic oxidation as anode；Obtain nickel oxalate@nickel foams；（3）By step（2）The nickel oxalate@nickel foams of preparation are placed on the centre of tube furnace, and sodium hypophosphite is placed on into tube furnace downstream, and under inert gas flow, setting temperature control program is：2~4 DEG C/min of heating rate, to after 380~450 DEG C, 2~4h is maintained, room temperature is then naturally cooled to, obtains nickel phosphide nano thin-film.The present invention first uses anodic oxidation, then is prepared for nickel phosphide nano thin-film by the method for low temperature phosphor, and compared with other methods, the present invention does not add any nickel source, the simple rapid and economical and effective of preparation method of the invention in preparation process. |
| priorityDate | 2016-03-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 50.