http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105777699-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D311-62 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D311-62 |
filingDate | 2016-05-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-11-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-11-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-105777699-B |
titleOfInvention | A kind of preparation method of non agricultural chemical residuum black rice anthocyanin |
abstract | Disclosed by the invention is the process that extraction purification prepares non agricultural chemical residuum anthocyanidin from black rice, and this method comprises the following steps:(1)Black rice extracts:Black rice raw material is taken, first adds raw material weight 5% 9%, the aqueous citric acid solution that mass fraction is 50 60%, it is 1 to be supplemented pure water to solid-liquid ratio:2‑1:3, after extracting 8 10 hours, coarse filtration, centrifugation, centrifugate using aperture as 0.5 micron of ceramic membrane filter, obtain filtrate again respectively;(2)Purifying:Purified using macroporous absorbent resin, eluted using the ethanol water that mass fraction is 40 60%;(3)Extraction:Extract and separate is carried out using the petroleum ether of 12 times of volumes, removes part residues of pesticides;(4)Silica gel column chromatography:Residues of pesticides are further removed through silica gel column chromatography;(5)Dry:Spray-dried that powdered black rice anthocyanin product is made, its anthocyanidin content is more than 30%, and residues of pesticides do not detect;Present invention process is simple, non agricultural chemical residuum, and anthocyanidin content is high, can fully meet the market demand, ensures food security. |
priorityDate | 2016-05-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 34.