Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_583d28bdec9bc0065ac0bcfb3a70731b |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C213-00 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C213-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C215-44 |
filingDate |
2015-12-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2fcd9a977723a1b2c93e7f5ea3fb45e3 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_528363eaa06b47dcde4653d314353526 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8668a247e94ecdae480fdab898fb4daf http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_310e63bafe4d2aa47d3eda6bf02e209c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_eb0f524ae15143db5ab16e35fd41599b |
publicationDate |
2016-06-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
CN-105712890-A |
titleOfInvention |
Purification technology of vildagliptin intermediate 3-amino-1-adamantanol |
abstract |
The invention discloses a purification technology of vildagliptin intermediate 3-amino-1-adamantanol. According to the purification technology, a water system (water, water-alcohol or water-toluene) is used, and methods of regulating acid for dissolving and regulating alkali for separating out are adopted, so that a 3-amino-1-adamantanol crude product can be purified. The purification technology is remarkable in purification effect and capable of controlling crystal forms precisely to facilitate raw control for preparing vildagliptin in next step. |
isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107325010-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114088849-A |
priorityDate |
2015-12-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |