http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105669828-A
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_04b7390d6bad30f3decdd01fc24fdfc2 |
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07K1-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07K1-16 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07K1-145 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07K1-16 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07K1-14 |
| filingDate | 2016-02-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8429f3c18787038f252b98de7d389f47 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_463b488b8a823af121246fafed9bc854 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a2ccf1eccbbb190f67b22f7b53337406 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6e792401710471d57d1d632d4a09b052 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6e24118a72726a8d41c4c7c527880397 |
| publicationDate | 2016-06-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-105669828-A |
| titleOfInvention | Preparation method of rape pollen enzymatic hydrolysis peptide |
| abstract | The invention discloses a preparation method which is used for breaking walls through a superfine smashing method for rape pollen enzymatic hydrolysis peptide and is easy to implement, free of water addition, high in wall breaking rate, free of solvent removal operation and beneficial to subsequent active component extraction. The method includes the steps of cleaning rape pollen, filtering away water, and adding low-boiling-point alcohol and other organic solvent according to a certain ratio for backflow three-time extraction. By means of the special vacuum, microwave and low-temperature drying device combined method, rape pollen extracts are dried, related active components are kept unchanged, drying temperature can be decreased, and drying speed can be increased. By means of the large-pore adsorption resin C18 reverse-phase silica gel column chromatography and specially-made chromatography combined technology, separation and purification are achieved, and a product with the rape pollen extract content of 90% is prepared. Furthermore, the purity of rape pollen extract recrystallized and extracted through a type of specific solvent prepared in our company reaches 95% or higher. Through orthogonal tests, the optimal process of extracting, drying, purifying and separating, and recrystallizing rape pollen extraction compound is determined. The preparation method is stable in process operation, high in extract yield, high in purity, free of environment pollution and suitable for meeting the requirement for modern industry automatic production. |
| isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114392292-A |
| priorityDate | 2016-02-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 88.