http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105665748-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B22F9-24 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B22F9-24 |
filingDate | 2016-04-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2018-01-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2018-01-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-105665748-B |
titleOfInvention | A kind of preparation method of high pure and ultra-fine silver powder |
abstract | The invention discloses a kind of preparation method of high pure and ultra-fine silver powder, comprise the following steps:A, silver nitrate crystal is purified;B, purification of chlorinated sodium crystal;C, silver nitride precipitation is prepared;D, silver nitride precipitation will be obtained in step c to be placed in the 4th container, then be continuously added NH into the 4th container 2 OHHCl hydrous ethanol solution is stirred continuously, until silver nitride precipitation all dissolves, reaction temperature is 20~25 DEG C, and mixing speed is 350~450r/min, there is the generation of suspension black solid on liquid level;E, filtering and under vacuum high pure and ultra-fine silver powder described in drying.The beneficial effects of the invention are as follows:Reaction prepares silver powder under the conditions of even phase, and granularity is small, particle is uniform;Dispersant need not be added, easily washing, silver powder purity is high;Ionic reaction is carried out in the solution, and contact area is big, and reaction speed is fast;React at ambient pressure, simple production process, cost is low;Contamination-free is discharged. |
priorityDate | 2016-04-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 42.