http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105646514-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D493-04 |
filingDate | 2014-11-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2018-02-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2018-02-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-105646514-B |
titleOfInvention | One kind synthesis 1,4:The method of 3,6 pairs of dewatering hexitol methyl ethers |
abstract | The invention discloses one kind synthesis 1,4:The method of 3,6 pairs of dewatering hexitol methyl ethers.With 1,4:3,6 pairs of dewatering hexitols are initiation material, and Isosorbide-5-Nitrae is generated as methylating reagent, in the presence of acidic etherified effect using methyl ether compound:3,6 pairs of dewatering hexitol methyl ethers.Wherein, Isosorbide-5-Nitrae:3,6 pairs of dewatering hexitol methyl ethers are selected from the mono-, di- methyl ether of isobide, isomannite and different iditol, preferably isosorbide, dimethyl ether, and the total recovery of isobide methyl ether is up to more than 80%.The present invention uses environmentally friendly acidic catalyst, high catalytic efficiency, avoids the generation of a large amount of halide salt accessory substances in traditional etherification method, and the corrosion problems caused by highly basic, there is provided a kind of new, efficient Isosorbide-5-Nitrae:3,6 pairs of dewatering hexitol methyl ether syntheti c routes, and realize environmental friendly catalysis etherification reaction. |
priorityDate | 2014-11-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 49.