http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105566141-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C231-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C227-18 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C269-06 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C237-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-12 |
filingDate | 2015-12-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2018-01-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2018-01-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-105566141-B |
titleOfInvention | A kind of preparation method of L-aminobutanedioic acid condensation product |
abstract | The present invention relates to technical field of organic synthesis, more particularly to a kind of preparation method of L-aminobutanedioic acid condensation product, the preparation method to comprise the following steps:(1) with alcohol esterification occurs for L-aminobutanedioic acid, obtains L-aminobutanedioic acid diester;(2) benzyl ester of Boc L aspartic acids 1 is reacted with L-aminobutanedioic acid diester, obtains condensation product;(3) condensation product is hydrolyzed, produces the L-aminobutanedioic acid condensation product.The present invention is using L-aminobutanedioic acid and the benzyl ester of Boc L aspartic acids 1 as raw material, through being esterified, being condensed, hydrolyzing, isolating and purifying to obtain the L-aminobutanedioic acid condensation product of high-purity.The preparation method is adapted to more large batch of preparation in laboratory, good impurity removing effect in purge process. |
priorityDate | 2015-12-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 53.