http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105460975-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2002-85 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2002-72 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2004-64 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2004-51 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2004-04 |
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01G30-002 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G30-00 |
| filingDate | 2015-12-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2017-12-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2017-12-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-105460975-B |
| titleOfInvention | Cu12Sb4S13The controllable method for preparing of nanocrystalline material |
| abstract | The invention belongs to nano material and field of nanometer technology, and in particular to Cu 12 Sb 4 S 13 The controllable method for preparing of nanocrystalline material, it is characterised in that comprise the following steps：1）It is 3 mmol by the adding proportion of cuprous iodide, antimony chloride, oleyl amine:1 mmol:10 mL, cuprous iodide and antimony chloride are added in oleyl amine, are passed through argon gas protective gas, control temperature and stirring is completely dissolved cuprous iodide and antimony chloride, obtain the complex solution of metal salt；2）The hexichol ethereal solution of the mol/L rhenocure CAs of 2 ~ 6 mL 1 is added in the complex solution of above-mentioned metal salt, is reacted after being heated to design temperature；3）After reaction terminates, room temperature is cooled to, adds the Cu that methanol obtains to reaction 12 Sb 4 S 13 It is nanocrystalline to be cleaned, obtain Cu 12 Sb 4 S 13 Nanocrystalline material.The preparation method technique is simple, and cost is cheap. |
| priorityDate | 2015-12-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 31.