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filingDate 2015-11-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2018-02-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2018-02-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-105369306-B
titleOfInvention A kind of preparation method of electro-catalysis water decomposition oxygen electrode
abstract Present invention relates particularly to the preparation method of a kind of Fe/Ni bimetallics and the electro-catalysis water decomposition oxygen electrode of the metal-organic framework materials of trimesic acid coordination, belong to electro-deposition/electro-catalysis field.Methods described step:(1) by Ni (NO 3 ) 2 ·6H 2 O、Fe(NO 3 ) 3 ·9H 2 O and trimesic acid are dissolved in N, in N dimethylformamides, add methyl tributyl ammonium sulfate methyl esters, are stirred well to after being completely dissolved, obtain the electrolyte of Fe/Ni bimetallics and the metal-organic framework materials of trimesic acid coordination;(2) using nickel foam as working electrode, using silver/silver chlorate saturation electrode as reference electrode, using platinized platinum as to electrode, to match somebody with somebody solution as electrolyte in step (1), it is assembled into the three-electrode system of standard;(3) three-electrode system of step (2) Plays is connected to electrochemical workstation, after carrying out constant potential electro-deposition, working electrode is taken out from electrolyte, cleans, dry, obtain described electro-catalysis water decomposition oxygen electrode.
priorityDate 2015-11-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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