http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105367692-B
Outgoing Links
Predicate | Object |
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classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08F2500-02 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08F2-26 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08F114-26 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F114-26 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F2-26 |
filingDate | 2015-12-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-11-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-11-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-105367692-B |
titleOfInvention | The preparation method of low molecular weight tetrafluoro ethylene resin |
abstract | A kind of preparation method of low molecular weight tetrafluoro ethylene resin is disclosed, it comprises the following steps:(1) in the presence of water and 500 5000ppm fluorine-containing surfactants, 200 1000ppm carboxylic acids or its salt, the anionic non-fluorinated surfactants of 100 1000ppm under 60 100 DEG C of temperature, 5 2.8MPa pressure polymerizing tetrafluoroethylene monomer 23 hours, obtain solid content be 10 30 weight % polytetrafluoroethyldispersions dispersions;The fluorine-containing surfactant is selected from C 2 F 5 OCF 2 CF 2 OCF 2 COONH 4 ;XCF 2 CF 2 (O)MCF 2 CF2OCF 2 COOA, wherein X are hydrogen or fluorine atom, and A is selected from hydrogen atom, alkali metal or ammonium ion;And CF 3 ‑(OCF 2 ) m ‑O‑CF 2 X, wherein m=1 3, X are hydroxy-acid group or its salt;The anionic non-fluorinated surfactant is selected from sulfonic acid type surfactant and sulfuric acid type surfactant;(2) inorganic acid is added into obtained polytetrafluoroethyldispersions dispersions, condenses polyflon;(3) neutralize, wash, and dry, obtain the polyflon of low molecule amount. |
priorityDate | 2015-12-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 70.