| Predicate |
Object |
| assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d9de52bba13e16028dffa8775e3f3f28
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_bf636e18b92762697899c27845ecd969 |
| classificationCPCAdditional |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02E60-10 |
| classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G73-1067
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/H01G11-30
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/H01M4-60
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G73-1003 |
| classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/H01M4-60
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/H01G11-30
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G73-10 |
| filingDate |
2015-09-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a8b51594a8e77ad7b06c275dd29e4c87
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c63126a2e022f6ebee47a9602bd73fc5
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_515e385cb1dbc0643a30bbfb4e9c903c
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d2f21467b6b4dd5e159db28afea79506
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_be07b159681a19c436944da3acde968c |
| publicationDate |
2016-02-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber |
CN-105295044-A |
| titleOfInvention |
Preparation method and application of macroporous covalent organic framework |
| abstract |
The invention provides a preparation method and application of a macroporous covalent organic framework. The structure of the macroporous covalent organic framework is as shown in a formula I; the preparation method of the macroporous covalent organic framework comprises the following steps of adding pyromellitic dianhydride and tris(4-(p-hydroxyphenyl)-phenyl)benzene into solvent, and dispersing to form a suspension, wherein the solvent is a mixed solvent of methylbenzene, dioxane and isoquinoline; performing liquid nitrogen freezing-vacuumizing-degassing treatment on the suspension for at least three times, sealing and carrying out microwave-assisted thermal reaction on the solvent at the temperature of 120DEG C to obtain a crude product; centrifuging the crude product, then collecting insoluble matters, and sequentially washing and drying with tetrahydrofuran and methylbenzene to obtain the macroporous covalent organic framework. The preparation method and the application provided by the invention have the beneficial effects that the method is pollution-free, mild and simple in reaction conditions and simple in requirement on the equipment, and is suitable for industrial large-scale production. |
| isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113912803-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108864435-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109627441-B
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109627441-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114016068-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109265464-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108503828-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106328391-A |
| priorityDate |
2015-09-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type |
http://data.epo.org/linked-data/def/patent/Publication |