http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105251418-B
Outgoing Links
Predicate | Object |
---|---|
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J13-00 |
filingDate | 2015-11-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-04-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-04-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-105251418-B |
titleOfInvention | Method for preparing Pickering microemulsion gel from poly-o-phenylenediamine |
abstract | The invention discloses a method for preparing Pickering microemulsion gel from poly-o-phenylenediamine. The method comprises the steps: 1, adding 0.5ml of an oil-phase solvent into 1.0ml of a 0.15-0.2mol/L o-phenylenediamine aqueous solution to obtain a solution, oscillating the solution, and performing ultrasound operation under the frequency being 60-80Hz for 10-20min until the solution becomes a milky-state turbid liquid; and 2, adding 5mu L of a 0.4-0.55mol/L FeCl3 solution under an ultrasound condition until yellow-green sediment is generated in the solution, further performing ultrasound operation for 10-20m, standing for reaction for 8-12d to obtain a product distributed on an oil-water interface in a gel state, and removing superfluous water-phase and oil-phase solutions to obtain the Pickering microemulsion gel containing the stable poly-o-phenylenediamine. The method is simple, high in repeatability and the universality, and suitable for a plurality of oil phases; and all the steps can be performed under room temperature, and heating is not required. |
priorityDate | 2015-11-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 28.