http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105237590-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H3-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H1-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H3-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H15-04 |
filingDate | 2015-09-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2018-12-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2018-12-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-105237590-B |
titleOfInvention | The method of one pot process alpha-glycosyl compound |
abstract | The invention discloses a kind of methods of one pot process alpha-glycosyl compound; glycosyl iodine with full TMS protection is sugared donor; monohydroxy TMS sugar is saccharide acceptor; using organic reagent as solvent, under special catalyst and phase transfer catalyst effect, 12h is stirred at room temperature in control; sugared donor and saccharide acceptor combine the single α-glucosides key connection oligosaccharides or sugar for generating full TMS protection to sew object; 40% acetic acid solution is added thereto again, TMS can be gone to protect, obtains tool α-glycosidic bond oligosaccharides or sugar sews object.Regioselectivity of the present invention is high, only obtain single α-glucosides key connection sugar compounds, a kind of new α-glycosidic bond synthetic method is provided, preferential catalyst is mild, it is cheap, be easy to get, be easy to handle, provide the guide's sugar compounds synthetic method of one kind rapidly and efficiently for sugared biological study research. |
priorityDate | 2015-09-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 57.