http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105233874-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D487-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J31-26 |
filingDate | 2013-11-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-07-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-07-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-105233874-B |
titleOfInvention | The technique that one-step method prepares porphyrin functionalized nano zinc sulphide |
abstract | The invention discloses the technique that one-step method prepares porphyrin functionalized nano zinc sulphide, step is as follows:Tetracarboxylic phenyl porphyrin is completely dissolved in the sodium hydroxide solution that pH is 89, the pH value for adjusting above-mentioned solution with a small amount of certain density hydrochloric acid solution is 67;Water-soluble zinc salt solution is prepared, is added in above-mentioned solution, is well mixed, obtains solution A;Then hydrochloric acid solution is added in a certain amount of thioacetamide and obtains solution B;Solution A and solution B are placed in the molten device of sealing simultaneously, reacted 12 24 hours under the conditions of being stirred at room temperature, then scrubbed drying obtains the nano-zinc sulfide complex of porphyrin functionalization.Compared with prior art, this method has that preparation technology is simple, easy to operate, low cost, and porphyrin consumption is few, reaction condition gentle and the advantages of high income;Have the advantages that purity height, size are small, active good using the nanometer sulfide of porphyrin functionalization made from this method. |
priorityDate | 2013-11-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 38.