http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105175356-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N27-48 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D285-135 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N27-48 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D285-135 |
filingDate | 2015-09-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-07-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-07-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-105175356-B |
titleOfInvention | Cup [4] aromatic hydrocarbons thiadiazoles derivative, cup [4] aromatic hydrocarbons thiadiazoles derivative multi-walled carbon nano-tubes compound and its preparation method and application |
abstract | The present invention relates to a kind of cup [4] aromatic hydrocarbons thiadiazoles derivative, cup [4] aromatic hydrocarbons thiadiazoles derivative multi-walled carbon nano-tubes compound and its preparation method and application.Being divided to two big steps is carried out, and be dissolved in anhydrous acetonitrile and acetone for the thiadiazoles of 2 amino, 5 sulfydryl 1,3,4- and Anhydrous potassium carbonate by the first step, oil bath agitating heating.After a period of time, cup [4] the aromatic hydrocarbons dibromo compound solution dissolved with acetonitrile is dividedly in some parts.Gained crude product is extracted, and is washed till neutrality, is dried, and filtering is isolated and purified.In the concentrated sulfuric acid and concentrated nitric acid be heated to reflux multi-walled carbon nano-tubes by second step, washing, and centrifugation is until weakly acidic pH, drying, backflow etc., finally obtain the calixarenes thiadiazoles derivative multi-walled carbon nano-tubes compound of black powder.The calixarenes thiadiazoles derivative carbon mano-tube composite prepared using the inventive method, shows excellent electronic conductivity energy and recognition capability, understands that the compound can determine copper trace by electrochemical method. |
priorityDate | 2015-09-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 64.